The Crystal Structure Of Saturated Bislactam

Authors : Gülten GÜNEL

Pages : 37-46

Doi:10.1501/commua1-2_0000000060

View : 11 | Download : 5

Publication Date : 1989-01-01

Article Type : Research Paper

Abstract :The crystal structure of saturated bislactam has been determined from three dimensional siııgle crystal X-ray data. The crystals are monolinic, with ımit-cell dimensions a = 43.431insert ignore into journalissuearticles values(2);, b— 7.707insert ignore into journalissuearticles values(1);, c— 13.586insert ignore into journalissuearticles values(1); Â, B -- 96.35insert ignore into journalissuearticles values(1);°, space group C2 / c and Z— 8. The structure was solved by dı’rect methods and refined by full-matrix least squares to R — 0.061 for the 3374 independent diffractometer measured reflections. The title compound forms a 1:1 inclusion compound with o-xylne and the molecules have almost perfect C2-symmetry uhich is a non- crys1 allograph ic symmetry.
Keywords : Crystal, Structure, Bislactam