SYNTHESIS AND THERMAL PROPERTIES OF NOVEL MALEONITRILES

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Sigma Mühendislik ve Fen Bilimleri Dergisi
Volume:34 Issue:2
SYNTHESIS AND THERMAL PROPERTIES OF NOVEL MALEONITRILES

SYNTHESIS AND THERMAL PROPERTIES OF NOVEL MALEONITRILES

Authors : Ali ERDOĞMUŞ

Pages : 153-158

View : 31 | Download : 11

Publication Date : 2016-06-01

Article Type : Research Paper

Abstract :In this study, the synthesis and thermal properties of two novel maleonitriles bearing 8-membered heterocyclic derivatives is described first time. New maleonitriles, benzo-insert ignore into journalissuearticles values(1,2-bis-methylthio);maleonitrile and [Benzo-15-crown-5]-insert ignore into journalissuearticles values(4,5-bis-methylthio);maleonitrile have been prepared by the reaction of different alkyl halides such as 1,2-bisinsert ignore into journalissuearticles values(brommethyl);benzene and 4,5-bis-insert ignore into journalissuearticles values(brommethyl);[benzo-15-crown-5] with dithiomaleonitrile disodium salt. Both compounds are characterized by IR, Mass, NMR spectroscopy as well as elemental analysis.
Keywords : Macrocycle, maleonitrile, crown ethers, thermal properties

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