Convenient synthesis of monomeric steroids from steroidal oxalate dimers using flash vacuum pyrolysis (FVP)

Authors : Lutfun NAHAR, Alan B Turner And Satyajit D SARKER

Pages : 359-366

Doi:10.3906/sag-1205-85

View : 16 | Download : 11

Publication Date : 0000-00-00

Article Type : Research Paper

Abstract :Flash vacuum pyrolysis insert ignore into journalissuearticles values(FVP); or thermolysis insert ignore into journalissuearticles values(FVT);, an environmentally friendly method for studying organic reaction mechanisms as well as synthesis, was applied to a series of oxalate dimers insert ignore into journalissuearticles values(1, 3, 5, 7, 9, 11, 13, and 15); to synthesise monomeric enes, dienes, and a triene insert ignore into journalissuearticles values(2, 4, 6, 8, 10, 12, 14, and 16);. All steroidal monomers were identified by spectroscopic means.
Keywords : Steroid, oxalate dimers, steroidal alkene, diene, triene, FVP