Synthesis, Characterization and Thermal Analysis of Organotin(IV) Derivatives of 4-(N-Maleoyl)Butanoate

Authors : Khadija SHAHID, Saqib ALI, Moazzam Hussain BHATTI

Pages : 589-598

View : 14 | Download : 11

Publication Date : 0000-00-00

Article Type : Research Paper

Abstract :Organotininsert ignore into journalissuearticles values(IV); derivatives of the type R4 - nSnLn where R = Me, n-Bu, Ph, L = 4 - insert ignore into journalissuearticles values(N-maleoyl);butanoate and n = 1 or 2 were synthesized by refluxing R3SnCl and R2SnCl2 with insert ignore into journalissuearticles values(4-insert ignore into journalissuearticles values(N-maleoyl);butanoate in the presence of triethylamine using dry toluene as solvent. These compounds were characterized by IR, multinuclear NMR and mass spectrometry. We also studied their thermal behavior and calculated the degradation pattern, energy of activation insert ignore into journalissuearticles values(Ea); and order of reaction insert ignore into journalissuearticles values(n);.
Keywords : Turk J Chem, 26, 2002, 589 598 Turk J Chem, vol 26, iss 4