Characterization and purification of 1,2,4-triazole-containing phthalocyanines synthesized by microwave method and structure elucidation by spectroscopic techniques

Authors : Asiye NAS, Ümit DEMİRBAŞ, Nurhan GÜMRÜKÇÜOĞLU, Halit KANTEKİN

Pages : 229-238

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Publication Date : 0000-00-00

Article Type : Research Paper

Abstract :The complexes of peripherally tetra-substituted metal-free insert ignore into journalissuearticles values(8);, leadinsert ignore into journalissuearticles values(II); 9);, and zincinsert ignore into journalissuearticles values(II); insert ignore into journalissuearticles values(10); phthalocyanine derivatives were synthesized for the first time in this work. The structures of these new complex compounds have been elucidated using many spectral methods such as electronic absorption, FT-IR, $^{1}$H NMR, $^{13}$C NMR, elemental analysis, and mass spectra. The thermogravimetric behavior of compounds 8-10 was determined by thermogravimetric analysis method in addition to these spectral methods.
Keywords : Metallophthalocyanine, 1, 2, 4 triazole, 4 nitrophthalonitrile, thermogravimetric analysis, ethyl 4 methylben zimidate